Test Specification Min Max TOTAL CAPSAICINOIDS (HPLC) AS REPORTED AS REPORTED CAPSAICIN (HPLC) 60.0 - 70.0% 60.0 - 70.0% CONTENT OF CAPSAICIN AND DIHYDROCAPSAICIN 75% MELTING RANGE (NOT TO EXCEED...

Test Specification Min Max APPEARANCE

Test Specification Min Max WATER 1.50% EXPIRATION DATE

Test Specification Min Max APPEARANCE

Test Specification Min Max ASSAY (DRIED BASIS) 99 101.00% MELTING RANGE (WITHIN 3�C) 159� 165�C pH OF A 1 IN 100 SOLUTION 4.2 5.2 LOSS ON DRYING 0.40% CHROMATOGRAPHIC IMPURITIES...

Test Specification Min Max SPECIFIC GRAVITY @ 25[dC 1.042 - 1.047 1.042 - 1.047

Test Specification Min Max ASSAY 17 % +/- 1.5 % 17 % +/- 1.5 % EXPIRATION DATE

Test Specification Min Max ASSAY (DRIED BASIS) 97 103.00% SPECIFIC ROTATION [a][@D@] +79 to +86 +79 to +86 CHROMATOGRAPHIC PURITY TO PASS TEST LOSS ON DRYING 1.00% RESIDUE ON IGNITION...

Test Specification Min Max ASSAY (DRIED BASIS) 97 102.50% MELTING RANGE (DRIED BASIS) 62.5� 66.0� CHROMATOGRAPHIC PURITY TO PASS TEST TO PASS TEST LOSS ON DRYING 1.00% RESIDUE ON IGNITION...

Test Specification Min Max ASSAY (C[@7@]H[@6@]O[@2@]) 99.5 100.50% SOLIDIFICATION POINT 121� 123�C LEAD 2.0 mg/k READILY CARBONIZABLE SUBSTANCES TO PASS TEST READILY OXIDIZABLE SUBSTANCES TO PASS TEST RESIDUE ON IGNITION...

Test Specification Min Max ASSAY (C[@6@]H[@5@]CH[@2@]OH) 99.00% COLOR (APHA) 20 RESIDUE AFTER IGNITION 0.01% ACETOPHENONE (C[@6@]H[@5@]COCH[@3@]) 0.02% BENZALDEHYDE (C[@6@]H[@5@]CHO) 0.01%

Test Specification Min Max ASSAY (DRIED BASIS) 97 103.00% SPECIFIC ROTATION [a][@D@] +120� to +128� +120� to +128� WATER DETERMINATION 4.00% RESIDUE ON IGNITION 0.20% ORDINARY IMPURITIES TO PASS TEST...

Test Specification Min Max ASSAY (C[@3@]H[@5@]NaO[@3@]) 58.8 61.20% pH OF SOLUTION @ 25[dC 5 9 CHLORIDE (Cl) 0.05% SULFATES (SO[@4@]) TO PASS TEST ELEMENTAL IMPURITIES AS REPORTED AS REPORTED SUGARS...

Test Specification Min Max ASSAY (DRIED BASIS) 97 102.00% SPECIFIC ROTATION [a][@D@] +97 to +103 +97 to +103 CHROMATOGRAPHIC PURITY TO PASS TEST TO PASS TEST LOSS ON DRYING 1.00%...

Test Specification Min Max ASSAY (ANHYDROUS BASIS) 98 101.00% MELTING RANGE 136� 139�C pH OF A 1 IN 100 SOLUTION 4 5.5 WATER DETERMINATION 1.00% RESIDUE ON IGNITION 0.20% ORGANIC...

Test Specification Min Max ASSAY (DRIED BASIS) 98 102.00% RESIDUE ON IGNITION 0.10% ELEMENTAL IMPURITIES: PLATINUM (Pt) AS REPORTED AS REPORTED FREE p-AMINOPHENOL 0.01% ORGANIC IMPURITIES TO PASS TEST TO...

Test Specification Min Max ASSAY (DRIED BASIS) 97 103.00% SPECIFIC ROTATION [a][@D@] +118 to +126 +118 to +126 LOSS ON DRYING 1.00% RESIDUE ON IGNITION 0.20% ORDINARY IMPURITIES TO PASS...

Test Specification Min Max TYPICAL ASSAY 99.50% 99.50% HEAVY METALS (as Pb) 5 ppm EXPIRATION DATE ABSORBANCE OF A 3% AQUEOUS SOLUTION: @ 450 nm 0.01 @ 280 nm 0.05...

Test Specification Min Max ASSAY 97% CHLORIDE (Cl) 0.00% COPPER (Cu) 0.00% INSOLUBLE MATTER 0.01% LEAD (Pb) 0.01% NICKEL (Ni) 0.10% ZINC (Zn) 0.02%

Test Specification Min Max APPEARANCE

Test Specification Min Max ASSAY 99% WATER 0.10%

Test Specification Min Max AVAILABLE CHLORINE APPROX. 65 % APPROX. 65 %

Test Specification Min Max ASSAY (DRIED BASIS) 98 102.00% SPECIFIC ROTATION, [a][@D@]25 -0.10 to +0.10� -0.10 to +0.10� LOSS ON DRYING 0.50% RESIDUE ON IGNITION 0.20% ORGANIC IMPURITIES TO PASS...

Test Specification Min Max EXPIRATION DATE

Test Specification Min Max ASSAY 99.50% COLOR 10 RESIDUE AFTER EVAPORATION 0.00% TITRABLE ACID 0.0001 meq TITRABLE BASE 0.0003 meq WATER 0.02% HEAVY METALS (as Pb) 1 ppm FREE HALOGENS...

Test Specification Min Max ASSAY 99.90% CHLORIDE 0.00% FLUORIDE 0.01% SULFATE 0.00% WATER 0.05%

Test Specification Min Max ASSAY 23.5 - 26.5 % 23.5 - 26.5 %

Test Specification Min Max APPEARANCE

Test Specification Min Max ASSAY {[-(CH[@3@])[@2@]SiO-]n} 90.5 99.00% CONTENT OF SILICON DIOXIDE 4 7.00% DEFOAMING ACTIVITY TO PASS TEST LOSS ON HEATING 18.00% ELEMENTAL IMPURITIES: NICKEL (Ni) AS REPORTED SILVER...

Test Specification Min Max ASSAY (Ca) 34 40.00% LOSS ON IGNITION 8.00% WATER-SOLUBLE SUBSTANCES 0.50% ACID-INSOLUBLE SUBSTANCES 0.20% CARBONATE (CO[@3@]) TO PASS TEST CHLORIDE (Cl) 0.14% FLUORIDE 75 ppm NITRATE...

Test Specification Min Max ASSAY (GC; C[@12@]H[@26@]O) 98.00% COLOR (APHA) 10 WATER 0.05%

Test Specification Min Max ASSAY (C[@2@]H[@5@]O[@2@]) 99.00% 99.00% SPECIFIC GRAVITY @ 20[d/20[dC 1.1151-1.1156 1.1151-1.1156 COLOR (Pt-Co) 10 DIETHYLENE GLYCOL 0.50% ACIDITY (as CH[@3@]COOH) 0.01% IRON (Fe) 0.00% CHLORIDE (Cl) NOT...

Test Specification Min Max ASSAY (DRIED BASIS) 98 100.50% LOSS ON DRYING 2.00% ACID-INSOLUBLE SUBSTANCES 0.20% FLUORIDE 0.01% ARSENIC (As) 3 ppm BARIUM TO PASS TEST LEAD (Pb) 3 ppm...

Test Specification Min Max ASSAY [Ca(OH)[@2@]] 95.00% ASSAY (CaCO[@3@]) 3.00% INSOLUBLE IN HCl 0.03% CHLORIDE (Cl) 0.03% SULFUR COMPOUNDS (as SO[@4@]) 0.10% HEAVY METALS (as Pb) 0.00% IRON (Fe) 0.05%...

Test Specification Min Max ASSAY 99.50% 99.50% FREEZING POINT 2.0 - 3.0 C 2.0 - 3.0 C COLOR (APHA) 10