Test Specification Min Max ABSORPTION MAX. (IN METHANOL) 607 nm EXPIRATION DATE

Test Specification Min Max ASSAY (DRIED BASIS) 97 103.00% LOSS ON DRYING 1.00% RESIDUE ON IGNITION 0.50% ELEMENTAL IMPURITIES: NICKEL (Ni) AS REPORTED AS REPORTED MOLYBDENUM (Mo) AS REPORTED AS...

Test Specification Min Max ASSAY 97%

Test Specification Min Max ASSAY 95% EXPIRATION DATE

Test Specification Min Max ACTIVITY 98.0 - 101.0 % 98.0 - 101.0 % HYDROCHLORIDE CONTENT 25 - 27 % 25 - 27 % MELTING POINT 188� -194�C 188� -194�C MOISTURE...

Test Specification Min Max WATER 30% MELTING POINT (DRY) 121 - 123 C 121 - 123 C INSOLUBLE AND RESINOUS MATTER 0.01% INSOLUBLE IN TOLUENE 0.10% SULFATE 0.10% RETEST DATE...

Test Specification Min Max APPEARANCE

Test Specification Min Max ACTIVITY 600 GDU/g 600 GDU/g MICROBIAL LIMITS: TO PASS TEST TO PASS TEST RETEST DATE

Test Specification Min Max ACTIVITY APPROX.5000 ug/g APPROX.5000 ug/g MOISTURE 4% MICROBIAL LIMITS: ESCHERICHIA COLI 10 CFU/g SALMONELLA NONE DETECTED RETEST DATE MANUFACTURE DATE APPEARANCE

Test Specification Min Max ACTIVITY (CMCase) ? CMC units/g ? CMC units/g ACTIVITY

Test Specification Min Max ASSAY 98% TURBIDITY Clear at 50mg / Clear at 50mg / Solubility (Color) Yellow Yellow RETEST DATE

Test Specification Min Max APPEARANCE

Test Specification Min Max ASSAY APPROX. 97 % APPROX. 97 % RETEST DATE

Test Specification Min Max PURITY (GC) 97% 97% SPECIFIC GRAVITY (20/20) 1.1080 - 1.1120 1.1080 - 1.1120 REFRACTIVE INDEX (n20/D) 1.4020 - 1.4050 1.4020 - 1.4050

Test Specification Min Max ASSAY 97.00% 97.00%

Test Specification Min Max APPEARANCE EXPIRATION DATE DATE OF MANUFACTURE

Test Specification Min Max PROTEASE ACTIVITY 75 U.S.P.UNITS/m 75 U.S.P.UNITS/m FAT 6% MICROBIAL LIMITS: TOTAL PLATE COUNT 10000/g ESCHERICHIA COLI NEGATIVE SALMONELLA NEGATIVE EXPIRATION DATE

Test Specification Min Max APPEARANCE EXPIRATION DATE DATE OF MANUFACTURE

Test Specification Min Max NO SPECIFICATIONS

Test Specification Min Max ASSAY (DRIED BASIS) 98 102.00% LOSS ON DRYING 0.30% RESIDUE ON IGNITION 0.30% CHLORIDE 0.05% SULFATE 0.03% IRON 30 ppm RELATED COMPOUNDS TO PASS TEST TO...

Test Specification Min Max ASSAY APPROX. 97 % APPROX. 97 %

Test Specification Min Max APPEARANCE

Test Specification Min Max ASSAY 99%

Test Specification Min Max ASSAY APPROX. 99 % APPROX. 99 %

Test Specification Min Max ABSORPTION MAX 660 (395) nm 660 (395) nm

Test Specification Min Max ASSAY 98%

Test Specification Min Max ASSAY 90%

Test Specification Min Max ASSAY APPROX. 99.9 % APPROX. 99.9 %

Test Specification Min Max APPEARANCE

Test Specification Min Max ASSAY 98.50% 98.50% REFRACTIVE INDEX (20�C, 589 nm) 1.55 1.553

Test Specification Min Max ASSAY (C[@7@]H[@7@]SO[@2@]Cl) 99% 99% MELTING POINT 67 - 69 C 67 - 69 C

Test Specification Min Max ASSAY 90.00% 90.00%

Test Specification Min Max ASSAY (by GC) 98% 98%

Test Specification Min Max ASSAY APPROX. 75% APPROX. 75%

Test Specification Min Max ASSAY (DRIED BASIS) APPROX. 98% APPROX. 98%

Test Specification Min Max ASSAY 98%